Scientech Corporation · TWSE:3583
Scientech — Technical Presentation (2013)
110 slides from Scientech's technical presentation, 2013
Slide 1: ini |
ini | FRR ISSRAR DARE Bl PES
Slide 2: What We Do
What We Do • Industries which we serve: Semiconductor (front-end, back-end and GaAs), FPD/LCD, LED, Solar Cell, Data Storage, • Scientific Instruments, General Industries…etc. • Business Scope: Agent/Distributer, Service and Manufacturing. 2
Slide 3: Scientech
Scientech • Company Establishment: 1979 • Capital: US$ 21 Million (NTD 600 Million) • Founder and CEO/President: H.L. Hsieh • 2013 March will be Listed Company 3
Slide 4: Locations in Taiwan
Locations in Taiwan Offices are located close to customers’ sites • Taipei – Scientech HQ (1979) • Linko Office (1999) • Huko Factory (2007) • Hsinchu Office (1990) • Taichung Office (1999) • Tainan Office (1999) • Kaohsiung Office (1987) 4
Slide 5: Locations in China
Locations in China • Beijing office (2004) • Tianjin office (2001) • Jinin office (2010) • Chongqing office (2010) • Wuhan office (2011) • Wuxi office (2003) • Shanghai Office Suzho u (2001) • Shenzhen (2011) • Quinming (2002) 5
Slide 6: 500 persons in total
500 persons in total • 40 persons in Administration • 22 persons in Scientific Instrument Division • 12 persons in General Industries Division • 197 persons in Wafer Reclaim Division • 125 persons in Semi/Opto. Division – 30 in sales/marketing, 95 in Service/Application • 101 persons in Equipment Mf
Slide 7: DANI Instruments
DANI Instruments Company Presentation Massimo Cazzaniga – DANI Instruments S.p.A.
Slide 8: DANI Instruments
DANI Instruments is the only European company designing, manufacturing and marketing GC and GC/MS instrumentation DANI Instruments
Slide 9: DANI Instruments
The company was established in 1975 by a group of experts in the field of analytical instrumentation. They have devoted their knowledge to the new gas chromatographic technique cooperating with the most prestigious Italian scientific institutes. Scientific experience together with managerial capabil
Slide 10: DANI means: Development in ANalytical Instrumentation
DANI has continued to implement innovative techniques by introducing in the market very reliable, extremely versatile and easy to use instruments that meet with the users’ real requirements. DANI has diversified its activities by entering in the field of molecular sensors which are developed and man
Slide 11: DANI Instruments - Milestones
1975: First DANI Gas Chromatograph GC 3200 1977: First DANI Head Space Sampler HSS 3640 1977: First DANI Capillary GC GC 3900 1981: Symposium of Hindelang 1981: Presentation of Programmable Temperature Vaporizer PTV 1985: Manufacturing Agreement with Hewlett Packard for 1985: Head Space Sampler HSS
Slide 12: DANI Instruments - Milestones
2000: Digital Gas Chromatograph GC1000 2nd Series 2000: Head Space Sampler HSS 86.50 2nd Series 2002: Thermal Desorber STD1000 2006: New MASTER Line 2006: Fast Gas Chromatograph MASTER GC 2006: Liquid Autosampler MASTER AS 2006: Thermal Desorber MASTER TD 2007: DANI GC Capillary Columns DN series 20
Slide 13: In the last years we run FAST
In the last 5 years we run FAST
Slide 14: DANI Instruments
DANI Instruments is the only company able to renew and design a complete line of new instruments in the last 4 years … 2007 2011 Master GC 2007 Master SHS Master AS 2009 Master TD Master DHS 2009 Master TOF DANI Instruments
Slide 15: DANI Instruments
… we approached the market with Total Solutions … DANI Instruments
Slide 16: MASTER TOF
A new concept of Time Of Flight GC-MS M ASTER TOF Tim e Of Flight GC/ M S Products Portfolio
Slide 17: MASTER DHS
A Dynamic approach to High Sensitivity Headspace Analysis M ASTER DHS Dynam ic Headspace Sam per Products Portfolio
Slide 18: Master SHS
Excellent precision with Extreme Simplicity M aster SHS Headspace Sam per Products Portfolio
Slide 19: MASTER TD
Ultimate Solution for High Sensitive Detection of Volatiles M ASTER TD Therm al Desorber Products Portfolio
Slide 20: HSS 86.50 Headspace Sampler
HSS 86.50 Headspace Sampler
Slide 21: Applications
… in the last 4 years we developed more than one hundred applications able to cover all the main industries … Applications Industries Applications TOF GCxGC TOF GC DHS TD HSS Analyzers Perfumes Aroma Profile X X Perfumes Allergens X X X Perfumes Pesticides X Cosmetics Aroma Profile X X Cosmetics All
Slide 22: Applications
… in the last 4 years we developed more than one hundred applications able to cover all the main industries … Applications Industries Applications TOF GCxGC TOF GC DHS TD HSS Analyzers Forensic Flame Retardants X Forensic Drugs X Forensic Blood Alcohol X X X Pharma Residual Solvents X X X Environmen
Slide 23: Applications
… in the last 4 years we developed more than one hundred applications able to cover all the main industries … Applications Industries Applications TOF GCxGC TOF GC DHS TD HSS Analyzers Chemicals Amines X Chemicals Glycol Ethers X Chemicals Nitrosamines X X Chemicals Dioxane in Water X X Chemicals Ac
Slide 24: MASTER GC Fast Gas Chromatograph
MASTER GC Fast Gas Chromatograph
Slide 25: Why MASTER GC
MASTER in … speed … repeatability and split flow linearity … sam ple introduction … sensitivity … selectivity … data acquisition … accessibility … flex ibility … m odularity … easy to use … com plete solutions … design Why MASTER GC
Slide 26: Master in speed
Master in … speed DANI MASTER GC is able to dramatically decrease sample run times in a wide range of GC applications. Faster than a conventional GC, DANI MASTER GC increases your analytical productivity with an excellent sensitivity. Necessary for Fast GC High oven temperature rates High carrier ga
Slide 27: MASTER GC – FAST GC
Hydrocarbons Oil Index – ISO 9377-2 [mV] Fast GC Total time 5 min Conventional GC 250 Total time 20 min 200 Voltage 150 3 4 5 100 1 10 2 6 8 9 7 50 0 5 10 15 20 Time [min.] MASTER GC – FAST GC
Slide 28: MASTER GC – FAST GC
Polyaromatic Hydrocarbons (PAHs) Fast GC Peak Identification Total time < 10 min 1 Naphthalene Conventional GC 2 Acenaphthylene 3 Acenaphthene Total time 27 min 4 Fluorene 5 Phenanthrene 6 Anthracene 7 Fluoranthene 8 Pyrene 9 Benzo (a) Anthracene 10 Chrysene 11 Benzo (b) fluoranthene 12 Benzo (k) fl
Slide 29: MASTER GC – FAST GC
Fatty Acid Methyl Esters (FAME) Conventional GC Fast GC Total time 50 min Total time < 13 min MASTER GC – FAST GC
Slide 30: Master in repeatability and split flow linearity
Master in … repeatability and split flow linearity A patent pending Digital Flow Control (DFC) combined with a digital control of oven temperature, assures an unsurpassed and verified repeatability and split flow linearity in both conventional and in fast gas chromatography. Retention Time SD C8 0.0
Slide 31: Master in sample introduction
Master in … sample introduction DANI MASTER GC supports a complete range of injectors such as the DANI PTV that ensures unprecedented sample integrity and supports the stringent timing requirements of FAST GC through a rapid cool down. DANI PTV, with its high heating speed rate and wide range of use
Slide 32: PTV Injector – Strengths
Injection technique Split-Splitless On-Column PTV Split x - x Splitless x - x Cold on column - x x Solvent split - x (modified) x Large volume - x (modified) x SPME - x (modified) PTV Injector – Strengths
Slide 33: PTV Injector – Strengths
Discrimination Effect comparison between split/splitless injector and PTV PTV Injector – Strengths
Slide 34: PTV Injector – Strengths
1,40 1,20 1,00 0,80 0,60 PTV 0,40 Split-splitless 0,20 0,00 C12 C16 C20 C24 C26 C32 C36 C40 Repeatability comparison between split/splitless injector and PTV PTV Injector – Strengths
Slide 35: PTV Injector – Strengths
Solvent Split injection eliminated peak distortions due to solvent PTV Injector – Strengths
Slide 36: Master in sensitivity: FID Detector
FID Detector MASTER GC Linear Dynamic Range > 106 Low Detection Limits < 1.6 pg carbon/sec Data Acquisition Range 300 Hz Master in … sensitivity DANI MASTER GC features a full range of highly sensitive detectors. Each detector includes a Digital Pressure Control (DPC) which allows digital setting of
Slide 37: Master in sensitivity: ECD Detector
ECD Detector MASTER GC Linear Dynamic Range > 104 Low Detection Limits < 6 fg/sec lindane Data Acquisition Range 300 Hz Master in … sensitivity DANI MASTER GC features a full range of highly sensitive detectors. Each detector includes a Digital Pressure Control (DPC) which allows digital setting of
Slide 38: Master in selectivity: FPD Detector
FPD Detector MASTER GC Linear Dynamic Range S > 103 P > 104 Low Detection Limits <40 pg sulphur/sec as dodecanethiol <0.4 pg phosphorous/sec as tributylphosphate Data Acquisition Range 300 Hz Master in … selectivity DANI selective detectors specifically eliminate matrix interferences while providing
Slide 39: Master in selectivity: NPD Detector
NPD Detector MASTER GC Linear Dynamic Range > 104 Low Detection Limits <0.6 pg nitrogen/sec as azobenzene <0.1 pg phosphorous/sec as malathion Master in … selectivity Data Acquisition Range 300 Hz DANI selective detectors specifically eliminate matrix interferences while providing maximum sensitivit
Slide 40: Master in data acquisition
Master in … data acquisition The detectors data acquisition rate is up to 300 Hz for better reproducibility and accuracy of chromatographic signals. Detector Data Acquisition Range FID 300 Hz ECD 300 Hz NPD 300 Hz FPD 300 Hz TCD 300 Hz micro TCD 300 Hz PID 300 Hz MASTER GC – Strengths
Slide 41: Master in accessibility, flexibility, modularity
Master in … accessibility An easy to the complete system allows a simple maintenance and an effective cost reduction. Master in … flexibility Gas sampling valves, auxiliary ovens, switching valves and other optional devices make DANI MASTER GC the most suitable gas chromatograph for the development
Slide 42: Master in easy to use
Master in … easy to use An intuitive Touch Screen interface controls both the GC and AS with an ultimate simplicity. MASTER GC – Strengths
Slide 43: Master in easy to use
Master in … easy to use A light inside the oven simplifies column installation. MASTER GC – Strengths
Slide 44: Master in complete solutions
Master in … complete solutions DANI MASTER GC with Headspace Sampler DANI HSS 86.50, Thermal Desorber DANI MASTER TD and the new MASTER DHS Dynamic Headspace Sampler cover a wide range of applications in environmental, chemicals, petrochemicals, pharmaceutical, food and beverages fields. The DANI MA
Slide 45: MASTER GC – Selling Points
• FAST Gas Chromatograph (Oven, Injectors, Detectors) • SPEED Gas Chromatograph (Oven) • NO DISCRIMINATION Gas Chromatograph (PTV) • FLOW Gas Chromatograph (DFC Digital Flow Control) • SENSITIVE Gas Chromatograph (Detectors) • TOUCH Gas Chromatograph (Touch Screen) • MODULAR Gas Chromatograph • FLEX
Slide 46: HSS 86.50 Technical Presentation
DANI Instruments HSS 86.50 Technical Presentation Massimo Cazzaniga – DANI Instruments S.p.A.
Slide 47: HSS 86.50 Head Space Sampler
A SCENT OF FUTURE HSS 86.50 Head Space Sampler
Slide 48: Head Space Technique
Indirect method to analyze volatile compounds in liquid or solid samples. Analysis of vapor phase in thermodynamic equilibrium with the sample, in a closed system. Head Space Technique
Slide 49: Head Space Technique
K= Cc/Cg Partition coefficient Equilibrium After equilibration, a part of the headspace gas is statically sampled by means of a loop or a syringe. Head Space Technique
Slide 50: Head Space Technique: Influence of heating time
Influence of heating time Equilibrium D[X]G≈0 Degradation Condition [X]G ∆T Heating Time Working at equilibrium means an higher sensitivity and an higher accuracy of the measure. Head Space Technique
Slide 51: When it is used
When the sample matrix can not be directly injected • solid sample • complex matrix • viscous or corrosive matrix i.e. : soil, plastics, fuel oil, fruit peel, paste… When it is used
Slide 52: Benefits of Head Space Analysis
• Clean technique • Little or no sample preparation • Analysis of substances that can not be directly injected into GC • More sensitive than liquid injection • Reduced or absent solvent peak • Gas chromatographic columns life increasing • Quantitative and good precision technique Benefits of Head Sp
Slide 53: Automatic Sampling
Automatic Sampling • Sample equilibration • Pressurization • Venting (Sample loop filling) • Injection Sampling phases
Slide 54: Sampling phases: Pressurization
STEP 1: PRESSURIZATION VENT CARRIER AUXILIARY GAS LOOP MANIFOLD TO GC SAMPLE VIAL OVEN Sampling phases
Slide 55: Sampling phases: Venting
STEP 2: VENTING VENT CARRIER AUXILIARY GAS LOOP MANIFOLD TO GC SAMPLE VIAL OVEN Sampling phases
Slide 56: Sampling phases: Injection
STEP 3: INJECTION VENT CARRIER AUXILIARY GAS LOOP MANIFOLD TO GC OVEN SAMPLE VIAL Sampling phases
Slide 57: Gas optimization
Carrier gas flow rate high enough to avoid peak broadening Auxiliary gas pressure high enough to completely fill the loop Higher auxiliary gas pressure will result in a useless sample dilution and lower sensitivity Gas optimization
Slide 58: Constant incubation time
A SCENT OF FUTURE —— =/incubation tem enne: = sampling Interval wee = Valving v Ry NT = Vial In viol jt = Tne ” _ i | t NV uy _= Vial ou vial @ Sm mae NY vial 3 i, v vial 4 . ZZ , vial 3 » ee” ae etc. fetta et tttatadetabete erp dd tty or oe ae | => 12345 10 20 30 40 min Constant incubation time
Slide 59: MHE - Applications
• VCM in PVC resin • Styrene in polymer • Ethylene in PET • Ethylene Oxide in sterilized material • Residual volatile solvents in pharmaceutical • Residual volatile solvents in packaging MHE - Applications
Slide 60: Solvents in Blood
Solvents in Blood 4 8 5000 1. MEK 2. Benzene 3. MIBK 4800 4. Toluene 7 9 5. MNBK 4600 6. Ethylbenzene 7. p-Xylene 8. 1-Butanol (ISTD) 4400 6 10 9. o-Xylene 10. Styrene 4200 2 5 4000 1 3 3800 0 5 10 15 20 Time (min) HSS 86.50 - Applications
Slide 61: Residual volatile solvents in pharmaceutical
Residual volatile solvents in pharmaceutical 1 3 4 1. Methylene Chloride 2. Chloroform 3. Benzene 2 4. Trichloroethylene 5. Dioxane 5 Standard solution at concentration corresponding to the maximum allowable USP limits for 100 mg sample HSS 86.50 - Applications
Slide 62: Drinking Water Analysis
Drinking Water Analysis ECD PID Static Headspace + PTV focusing HSS 86.50 - Applications
Slide 63: Anaesthetics in biological fluids
Anaesthetics in biological fluids 4 1. Nitrous Oxide 2. Enflurane 3. Isoflurane 2 4. Halotane 1 3 HSS 86.50 - Applications
Slide 64: Determination of dioxane in water
Determination of dioxane in water Sample: Dioxane in water 10ppm HEAD SPACE SAMPLER PARAMETERS GAS CHROMATOGRAPH PARAMETERS Manifold: 150°C Oven: 50°C, 4 min, 25°C/min, 200°C, 3 min Oven: 85°C Injector: SL/IN, 180°C Transfer Line: 150°C Carrier gas: Helium, 10 mL/min, constant flow Incubation Time:
Slide 65: Residual solvents in food packaging using static headspace
Determination of residual solvents in food packaging using STATIC Headspace Peak Identification 1 ethanol 2 isopropanol 3 ethylacetate 4 metossipropanol 5 n-propilacetate 6 acetyl acetone 7 butylcellosolve Sample: 0.5 dm2 HEAD SPACE SAMPLER PARAMETERS GAS CHROMATOGRAPH PARAMETERS Oven: 50°C, 5min, 5
Slide 66: Determination of BTX and Styrene in water
Determination of BTX and Styrene in water using static headspace [mV] 12 styrene Sample: etylbenzene o-xylene toluene m-xylene p-xylene benzene 11 BTX and Styrene 10 in water 10 ppb Voltage 9 8 7 5 10 15 20 [min.] Time GAS CHROMATOGRAPH PARAMETERS HEAD SPACE SAMPLER PARAMETERS Oven: 40°C, 5°C/min, 1
Slide 67: Residual solvents in radiopharmaceuticals according to USP 467
Determination of residual solvents in radiopharmaceuticals using Head Space sampling technique According to USP 467 HEAD SPACE SAMPLER PARAMETERS Manifold: 95°C Oven: 95°C Transfer Line: 95°C Incubation Time: 30min. Aux Gas: He 0.7 bar Vent: 10 sec Sampling: 10 sec Press: 10 sec Sample: 5 ml GAS CHR
Slide 68: Determination of blood alcohol
DETERMINATION OF BLOOD ALCOHOL ALC 1 Methanol Acethaldehyde Ethanol 2-propanol Acetone +Acetonitrile MEK Ethyl acetate ALC 2 Acethaldehyde Methanol Ethanol press-fit Acetone FID 1 FID 2 2-propanol Acetonitrile Ethyl acetate column 1 MEK HSS 86.50 Conditions GC Conditions Oven: 60°C Oven: 35°C Manifo
Slide 69: HSS 86.50 - Fields of application
• Plastic industry – Acetaldehyde determination in polymers • Pharmaceutical industry – Residual volatile solvents in pharmaceutical • Food industry – Flavours in food • Clinical chemistry – Alcohols and organics in biological fluids • Industrial quality control – Ethylene oxide in sterilized produc
Slide 70: HSS 86.50 - Specifications
HSS 86.50 Sampling Method Valve&Loop Sample Capacity 44 Sample Vials 20ml or 10ml Sampling Device Temperature 45°C to 200°C Sample Pathway inert deactivated Sampling Volume 0,5 – 1 – 3 ml Incubation Oven Sample Capacity 6 Incubation Oven Temperature 40°C to 200°C Incubation Oven Time 1 to 300 min Vi
Slide 71: HSS 86.50 - Specifications
HSS 86.50 Automatic parameter increment YES Valve electrically actuated Methods stored 4 Dimensions 420x474x617mm (WxHxD) Weight 32Kg Power supply 220V (± 10%), 50Hz, 600VA Environmental conditions temperature 10 - 45°C humidity 0 - 95% HSS 86.50 - Specifications
Slide 72: What do you need for your analysis?
What do you need for your analysis?
Slide 73: Transfer Line Needles
TRANSFER LINE NEEDLES Description Set of Code Transfer Line needle - 0.7x0.4 2 pieces 2322.590 105 HSS 86.50 - HSS1000 Puntale Linea di Trasferimento - 0.7x0.4 2 pezzi Transfer Line needle - 0.5x0.2 2 pieces 2322.590 104 HSS 86.50 - HSS1000 Puntale Linea di Trasferimento - 0.5x0.2 2 pezzi 2322.590 1
Slide 74: Head Space Vials
HEAD SPACE VIALS Description Set of Code Vial 23x46 – volume 10 ml – crimp top 50 pieces 1262.195 001 HSS 86.50 - HSS1000 Vial 23x46 – volume 10 ml – chiusura a capsula 50 pezzi Vial 23x46 – volume 10 ml – crimp top 500 pieces 1262.020 003 HSS 86.50 - HSS1000 Vial 23x46 – volume 10 ml – chiusura a c
Slide 75: Description Set of Code
Description Set of Code Hand Crimper for crimp seal cod. 1260.895 002 1 piece 1343.000 007 HSS 86.50 - HSS1000 - SPT 37.50 Pinza Chiudi Vials per Capsula cod. 1260.895 002 1 pezzo Vials extractor for Vial 23x75 1 piece 1343.000 003 SPT 37.50 Estrattore per Vial 23x75 1 pezzo Tray adapter for Vial vo
Slide 76: Static Headspace Sampler SHS - International Sales Meeting
I nternational Sales M eeting April 5 th – 6 th 2011 Static Headspace Sampler SHS The Authentic Static Haedspace Sampler I laria Ferrante GC P roduct M anager
Slide 77: Static Headspace Sampler SHS: Historically The Best
Static Headspace Sampler SHS The FIRST universal headspace OVER three-decades of experience THE HEADSPACE’s NAME IS OVER 20000 Headspace produced Hystorically DANI The Best!
Slide 78: MASTER SHS designed with our customer in mind
Static Headspace Sampler SHS MASTER SHS designed with our customer in mind flexible system to meet all needs robust and trouble free design
Slide 79: Why a Static Headspace Sampler?
Static Headspace Sampler SHS ROBUST & FLEXIBLE TECNIQUE PROVEN & SENSITIVE TECHNIQUE UNIVERSAL COMPATIBILITY OUTSTANDING REPRODUCIBILITY Why a Static Headspace Sampler ? HIGHEST PRODUCTIVITY ACCURACY & DATA TRACEABILITY ENVIROMENTALLY SAFE Why a Static Headspace Sampler ?
Slide 80: Robust & Flexible Technique
Static Head Space Sampler SHS Static HeadSpace sampling technique is the most commonly used technique for the analysis of volatile and semivolatile compounds ROBUST & FLEXIBLE TECHNIQUE
Slide 81: Proven Sensitive Technique
Static Head Space Sampler SHS Sample flow path is entirely chemical inert ( Silconert 2000) Eliminated analytical carryover High temperature headspace sampler (300°C) Working at equilibrium means an higher sensitivity and a higher accuracy of the measure PROVEN SENSITIVE TECHNIQUE
Slide 82: Outstanding Reproducibility
Static Head Space Sampler SHS Valve & Loop is the most reliable and robust technique Compact manifold design ensures maximum thermal control Carrier gas flow rate is uninterruptedly maintained OUTSTANDING REPRODUCIBILITY
Slide 83: Outstanding Reproducibility: Step 1
Static Head Space Sampler SHS VENT CARRIER AUXILIARY GAS LOOP MANIFOLD TO GC Sampling phases STEP 1: SAMPLE OVEN VIAL Shaking Leak Check Pressurization OUTSTANDING REPRODUCIBILITY
Slide 84: Outstanding Reproducibility: Step 2
Static Head Space Sampler SHS VENT CARRIER AUXILIARY GAS LOOP MANIFOLD TO GC Sampling phases SAMPLE STEP 2: Venting VIAL OVEN OUTSTANDING REPRODUCIBILITY
Slide 85: Outstanding Reproducibility: Step 3
Static Head Space Sampler SHS VENT CARRIER AUXILIARY GAS LOOP MANIFOLD TO GC Sampling phases SAMPLE STEP 3: Injection VIAL OVEN OUTSTANDING REPRODUCIBILITY
Slide 86: Highest Productivity
Static Head Space Sampler SHS Up to 120 vial positions 18 vials oven capacity for maximized sample throughput Unilimited priority vial Maximum compatibility with headspace vials of 10 mL, 20 mL, 22 mL to meet every application need HIGHEST PRODUCTIVITY
Slide 87: Highest Productivity: Multiple Headspace Extraction
Static Head Space Sampler SHS NO need of External Standard Multiple HeadSpace Extraction (MHE) Quantitative method for complex matrices that eliminates sample matrix effect and allows to obtain the total peak area proportional to the total amount of analyte of the original sample and a consequent mo
Slide 88: Highest Productivity: Multiple Headspace Injection
Static Head Space Sampler SHS Sample too diluited Multiple HeadSpace Injection (MHI) allows a multiple valve&loop injection in a proper programmable temperature injector filled with dedicated sorbent material in order to improve the analytical system sensitivity. HIGHEST PRODUCTIVITY
Slide 89: Highest Productivity: Method Development Optimization
Static Head Space Sampler SHS New Analisys Method Method Development Optimization (MDO) any single method can be associated with an optimization procedure, in which the value of a selected parameter is automatically incremented of a constant amount in a series of consecutive samplings of identical s
Slide 90: Accuracy & Data Traceability
Static Head Space Sampler SHS Bar Code Reader guarantees sample ratification and validation, assuring data traceability Automatic Leak Check procedure ensures the proper pressurization and the perfect seal of each vial Sample tray cooling device preserves sample integrity CFR 21 Part 11 compliance A
Slide 91: Accuracy & Data Traceability
Static Head Space Sampler SHS Full controlled by Touch Scrren and SHS Manager SW or Clarity data station. ACCURACY & DATA TRACEABILITY
Slide 92: Accuracy & Data Traceability: IQ OQ / PQ Procedure
Static Head Space Sampler SHS IQ OQ / PQ Procedure [V] 2,52 Dichlorobenzene 1,0 2,71 Nitrobenzene 0,8 0,6 Voltage 0,4 0,2 0,0 0 1 2 3 4 5 Time [min.] Example of analysis with SL/IN - FID configuration ACCURACY & DATA TRACEABILITY
Slide 93: Universal Compatibility
Static Head Space Sampler SHS Easy connection with any kind of GC or GCMS system UNIVERSAL COMPATIBILITY
Slide 94: Environmentally Safe
Static Head Space Sampler SHS Headspace sampling technique is a Totally Green procedure, there is no need of solvents Gas Saving Function Tim e & Energy Saving Function Tw o separate pneum atic circuit for Aux iliary and carrier gas ENVIROMENTALLY SAFE
Slide 95: Wide range of applications
Static Headspace Sampler SHS WIDE RANGE OF APPLICATIONS Limited or no sample preparation No contamination risk Reduced inlet and column maintenance Analysis of substances that can not be directly injected into GC It is a very flexible technique suitable for solid and liquid sample matrices
Slide 96: SHS application fields
Static Headspace Sampler SHS FORENSIC PHARMACEUTICAL ENVIRONMENTAL PACKAGING FOOD & BEVERAGE POLYMERS BIODIESEL
Slide 97: Determination of blood alcohol
Static Headspace Sampler SHS DETERMINATION OF BLOOD ALCOHOL ALC 2 ALC 1 Acethaldehyde Methanol Methanol Acethaldehyde Ethanol Ethanol Acetone 2-propanol 2-propanol Acetone+ Acetonitrile Acetonitrile MEK Ethyl acetate Ethyl acetate MEK Master SHS Conditions Master GC GC Conditions Oven: 60°C Oven: 35
Slide 98: Determination of blood alcohol
Static Headspace Sampler SHS DETERMINATION OF BLOOD ALCOHOL Ethanol Linearity Carryover Calculated 700 DB-ALC1 = 0.006% 2 DB-ALC2= 0.012% 600 R = 0,9995 500 response (mV x s) 400 300 LOD = 93 ppb 200 100 0 0 500 1000 1500 2000 2500 3000 3500 concentration (ppm) FORENSIC
Slide 99: Residual volatile solvents in pharmaceutical USP 467
Static Headspace Sampler SHS RESIDUAL VOLATILE SOLVENTS IN PHARMACEUTICAL USP 467 PHARMACEUTICAL
Slide 100: Residual volatile solvents in pharmaceutical USP 467
Static Headspace Sampler SHS RESIDUAL VOLATILE SOLVENTS IN PHARMACEUTICAL USP 467 Master SHS complies with USP 467 method where is specifically required a Headspace system. PHARMACEUTICAL
Slide 101: Determination of BTEX and styrene in water
Static Headspace Sampler SHS DETERMINATION OF BTEX AND STYRENE IN WATER Master SHS Conditions Oven: 60°C Manifold: 70°C Tube: 80°C Press: 11.8 psi Incubation time:15 min. GC Conditions Oven: 35°C Inj: SL/IN 150°C Det: FID 300°C Carrier: He 18.8 psi Split: 1:5 ENVIRONMENTAL
Slide 102: Determination of BTEX and styrene in water
Static Headspace Sampler SHS DETERMINATION OF BTEX AND STYRENE IN WATER benzene toluene ethylbenzene p-xylene m-xylene o-xylene styrene average 22,02 26,04 28,65 28,67 29,28 24,94 20,38 devstd 0,28 0,20 0,41 0,34 0,25 0,27 0,19 RSD% 1,27 0,77 1,43 1,19 0,86 1,07 0,92 ENVIRONMENTAL
Slide 103: EPA Method Compliance
Static Headspace Sampler SHS DETERMINATION OF BTEX AND STYRENE IN WATER EPA Method Compliance Master SHS is perfectly compliances with EPA Method where is required a Headspace system. Preparative method EPA 5021 ( EPA 624, EPA 8260, etc….) Analitycal method EPA 8021 ENVIRONMENTAL
Slide 104: Residual solvents in food packaging
Static Headspace Sampler SHS RESIDUAL SOLVENTS IN FOOD PACKAGING 1 Methanol 2 Ethanol 3 2-Propanol 4 Acetone 5 Methylacetate 6 1-propanol 7 Sec-Butanol 8 2-Butanone 9 Ethylacetate 10 Isobutanol 11 THF 12 2-Methoxyethanol 13 Cyclohexane 14 isoproylacetate 15 n-Butanol 16 1-Methoxy-2-propanol 17 n-pro
Slide 105: Residual solvents in food packaging
Static Headspace Sampler SHS RESIDUAL SOLVENTS IN FOOD PACKAGING R2 Methanol 1,0000 Ethanol 0,9999 2-Propanol 0,9948 Acetone 0,9967 Methylacetate 0,9995 1-propanol 0,9973 Sec-Butanol 0,9994 2-Butanone 0,9905 Ethylacetate 0,9989 Isobutanol 0,9939 THF 0,9989 2-Methoxyethanol 0,9994 Cyclohexane 0,9990
Slide 106: Fruit fragrances: Strawberries profile
Static Headspace Sampler SHS FRUIT FRAGRANCES Strawberries Profile 9gr of sample in 10ml vial Master SHS Conditions Oven: 60°C Manifold: 150°C TrLine: 190°C Press: 0.64bar Incubation time:60 min. FOOD & BEVERAGE
Slide 107: Fruit fragrances: Banana profile
Static Headspace Sampler SHS FRUIT FRAGRANCES Banana Profile 6gr of sample in 10ml vial Master SHS Conditions Oven: 60°C Manifold: 150°C TrLine: 190°C Press: 0.64bar Incubation time:60 min. FOOD & BEVERAGE
Slide 108: Biodiesel: UNI EN ISO 14110
Static Headspace Sampler SHS UNI EN ISO 14110: 2003 GAS CHROMATOGRAPH PARAMETERS Oven: 70°C, 20 min Injector: SL/IN 150°C Carrier gas: Helium, 1 mL/min, constant flow Injection mode: split, 50ml/min. Detector: FID, 150°C Column: DN-BioDiesel : 30 m, 0.32 mm, 1 µm Sample: standard mixture of methanol
Slide 109: Conclusions
C ONCLUSI ONS The most used technique in the field of VOC analisys Utilized for liquid and solid sample Easy to use Fully automated Versatile MASTER SHS THE DANI SOLUTION FOR HEADSPACE ANALIYSIS CONCLUSIONS
Slide 110: www.scientech.com.tw
A SCENT OF FUTURE mae PE www.scientech.com.tw